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2 article(s) from Volkmer, Dirk

Long-term entrapment and temperature-controlled-release of SF₆ gas in metal–organic frameworks (MOFs)

Hana Bunzen,
Andreas Kalytta-Mewes,
Leo van Wüllen and
Dirk Volkmer

Beilstein J. Nanotechnol. 2019, 10, 1851–1859, doi:10.3762/bjnano.10.180

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Scheme 1: Synthesis of MFU-4.

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Figure 1: Thermogravimetric analysis of MFU-4 before (black) and after (Sample 3a, blue) the loading of SF₆ m...

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Figure 2: FTIR spectra of MFU-4 before (black) and after (Sample 3a, blue) the loading of SF₆. Bands attribut...

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Figure 3: Powder X-ray diffraction analysis of MFU-4 before (black) and after (Sample 3a, blue) the loading o...

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Figure 4: ¹⁹F MAS NMR spectrum of MFU-4 (Sample 3b) loaded with SF₆ recorded at room temperature. The spectru...

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Figure 5: (a) MFU-4 unit cell showing the linear transition scan path for SF₆ crossing a single small pore. (...

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Figure 6: Thermogravimetric analysis of MFU-4 loaded with SF₆ (Sample 3a) after 0, 1, 3, 7, 14, and 60 days m...

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Figure 7: FTIR spectra of MFU-4 loaded with SF₆ (Sample 3a) after 0, 1, 3, 7, 14, and 60 days. Bands attribut...

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Full Research Paper

Published 10 Sep 2019

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Preparation of thick silica coatings on carbon fibers with fine-structured silica nanotubes induced by a self-assembly process

Benjamin Baumgärtner,
Hendrik Möller,
Thomas Neumann and
Dirk Volkmer

Beilstein J. Nanotechnol. 2017, 8, 1145–1155, doi:10.3762/bjnano.8.116

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Figure 1: Schematic illustration of the covalent linkage of tetraethylenepentamine to carbon fibers via wet-c...

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Figure 2: Transmission electron micrograph of thin silica shells remaining after calcination of the TEPA-modi...

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Figure 3: Atomic force micrographs of carbon fibers after 40 min in 30 vol % TMOS solutions with a pretreatme...

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Figure 4: a) Scanning and b) transmission electron micrograph of mineralized LPEI aggregates.

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Figure 5: Schematic illustration of LPEI mediated silicification of carbon fibers: a) chopped carbon fibers a...

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Figure 6: Scanning electron micrographs of a) a carbon fiber coated with a silica shell mediated by LPEI (ins...

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Figure 7: Scanning electron micrographs of mineralized LPEI aggregates modified by copper nitrate addition, a...

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Figure 8: Scanning electron micrograph of mineralized LPEI aggregates modified by calcium nitrate addition.

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Figure 9: Scanning electron micrographs of carbon fibers coated with a silica shell mediated by LPEI with add...

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Figure 10: Scanning electron micrograph of a carbon felt with a LPEI mediated silica coating. Inset: photograp...

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Figure 11: Scanning electron micrograph of silicon carbide fibers coated with a silica shell mediated by LPEI.

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Full Research Paper

Published 26 May 2017

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Long-term entrapment and temperature-controlled-release of SF6 gas in metal–organic frameworks (MOFs)

Preparation of thick silica coatings on carbon fibers with fine-structured silica nanotubes induced by a self-assembly process

Long-term entrapment and temperature-controlled-release of SF₆ gas in metal–organic frameworks (MOFs)